Analytical methods for mercury analysis According to US EPA, list of many of the regulatory methods that are available for use with today’s technologies. Most all environmental methyl mercury analyses is a variation on the … We routinely analyze water, biological matter and soils. Industrial hygienists must monitor the naturally occurring mercury levels emanating from crude oil wells and processing plants. It is applicable to drinking water, surface and ground waters, marine water, and industrial and municipal wastewater. With 10 ICP-MS’s and 4 CVAFS system for mercury analysis and speciation, we have the capacity to offer very fast 24-48 hour turnaround times when needed for most analyses. Transportable analysers. atomic fluorescence spectrometry (CVAFS). The Method is similar to EPA Method 1631, Mercury in Water by Oxidation, Purge and Trap, and Determination of Mercury in Aqueous and Geologic Materials (CVAFS) —Techniques and Methods 5–D2 Techniques and Methods 5–D2 U.S. Department of the Interior ... (all matrices) for mercury analysis because contamination of either the sample or the sampling equipment is possible due to the ubiquitous nature of mercury in the environment. 3.0 Safety Issues: Specific safety concerns for each chemical can be found in the Material Safety Data Sheets for that chemical, all of which are located in the laboratory. 3. The mercury vapor is thermally desorbed to a second gold trap (analytical) and from that detected by cold vapor atomic fluorescence spectrometry (CVAFS). Analysis of Mercury by ICP-MS Mercury (Hg) is a rare heavy metal, many forms of which are highly toxic by inhalation, ingestion or absorption through the skin. Comparisons between CVAAS and CVAFS for mercury analysis generally show good comparability with low experimental biases, especially if interfering species are absent [ ]. Although the detector can be run using nitrogen as a carrier, sensitivity drops by 50 to 75% compared to argon. It was designed to be easy to set up, easy to use, and easy to maintain. Direct injection in a closed system flow design ensures no loss of volatile analytes, providing uncompromised precision and … The large working range of the system allows for analysis at the ultra-trace level up to very high concentrations. 3.2. Mercury, Low Level (EPA Method 1631, AFS) Eurofins TestAmerica developed a Low Level Mercury Analysis following EPA Method 1631 in 2002. Virtually any molecular species in the carrier gas suppress the output signal. The purge and trap CVAFS is an extremely sensitive method for mercury analysis. Samples high in organic matter may require initial pretreatment in an ultra violet (UV) digester to remove the colour associated with the organic matter. Our patented dual pure-gold cartridges and ultra-stable CVAFS detector provide unmatched accuracy, sensitivity and … Scope and application: Method 245.7 is for determination of mercury (Hg) in filtered and unfiltered water by cold-vapor atomic fluorescence spectrometry (CVAFS). The Tekran ® 2700 Methyl Mercury Analysis System offers an automated solution for complex and time consuming manual techniques. A detection limit (3σ) of 0.016 ng/l for MeHg analysis in water samples has been reported . Cold Vapour Atomic Absorption Spectroscopy (CVAAS): Cold Vapour At omic Fluorescence Spectroscopy (CVAFS): Direct Analysis by Thermal Decomposition: ICP or ICP-MS: 07/23/17 15 Each technique has advantages and disadvantages, I'll review each technique and provide tips for choosing the right one for various situations. 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